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• W3107488370 abstract "A combined electrochemical and electron paramagnetic resonance (EPR) procedure for the study of oxygen reduction reaction (ORR) intermediates generated at Pt nanoparticles (NPs) is validated in this work. Using spin-trap EPR complemented by electrochemical analysis, we show that we can detect and identify the free radicals that are produced during the ORR through trapping with 5,5-dimethyl-1-pyrroline-N-oxide (DMPO) which are otherwise difficult to detect. Experiments with 5-(diethoxyphosphoryl)-5-methyl-1-pyrroline-N-oxide (DEPMPO) as spin trap show no evidence of DEPMPO-OOH and indicate that only OH radicals are trapped during the ORR. The results of this study serve as a functional proof-of-concept for further research on the identification of radical ORR intermediates in solution. We propose that our procedure can be used for a more rigorous quantification of free radicals involved in other electrochemical reactions." @default.
• W3107488370 created "2020-12-07" @default.
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• W3107488370 date "2021-01-01" @default.
• W3107488370 modified "2023-10-09" @default.
• W3107488370 title "Reactive oxygen species formation at Pt nanoparticles revisited by electron paramagnetic resonance and electrochemical analysis" @default.
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• W3107488370 doi "https://doi.org/10.1016/j.elecom.2020.106878" @default.
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