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• W3108664504 abstract "Abstract Inorganic, lead‐free metal halides are widely sought after following the rise of the halide perovskites as outstanding optoelectronic materials, due to their enhanced stability and reduced toxicity. Herein, we report on the solvothermal synthesis of Rb 7 Sb 3 Br 16 , which exhibits a 0D structure comprised of [SbBr 6 ] 3− octahedra and edge‐sharing bioctahedra [Sb 2 Br 10 ] 4− dimers that order into layers along the c ‐axis. This all‐inorganic material is air‐stable and exhibits weak orange photoluminescence (PL) at room temperature. Low‐temperature PL and PL excitation (PLE) measurements reveal the presence of two distinct emission bands that originate from these structural units, with the high‐energy emission quenching as temperature rises beyond 150 K. We are also able to obtain Rb 7 Bi 3 Br 16 and Rb 7 Bi 3 I 16 which both crystallize in orthorhombic symmetry, with Rb 7 Bi 3 Br 16 presenting weak low‐temperature luminescence while Rb 7 Bi 3 I 16 is non‐luminescent. This work expands the library of emissive inorganic metal halides and provides further evidence for the efficacy of low‐dimensional Sb−X luminescent centers based on octahedral and edge‐sharing [Sb 2 X 10 ] 4− dimers." @default.
• W3108664504 created "2020-12-07" @default.
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• W3108664504 date "2020-12-14" @default.
• W3108664504 modified "2023-09-25" @default.
• W3108664504 title "Expanding the 0D Rb₇M₃X₁₆ (M=Sb, Bi; X=Br, I) Family: Dual‐Band Luminescence in Rb₇Sb₃Br₁₆" @default.
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• W3108664504 doi "https://doi.org/10.1002/hlca.202000206" @default.
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