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- W3109625971 abstract "The qualitative analysis of nanodiamonds by FTIR spectrometry as photoacoustic (FTIR–PAS), diffuse-reflectance (DRIFT), and attenuated total reflection (ATR) modalities was evaluated for rapid and nondestructive analysis and comparison of nanodiamonds. The reproducibility and signal-gathering depth of spectra was compared. The assignment of characteristic bands showed that only six groups of bands were present in spectra of all the modalities with appropriate sensitivity: 1760 (C=O stretch, isolated carboxyl groups); 1640–1632 (H–O–H bend, liquid water); 1400–1370 (non-carboxyl C–O–H in-plane bend and CH2 deformation); 1103 (non-carboxyl C–O stretch); 1060 (in-plane C–H bend, non-aromatic hydrocarbons and carbohydrates); 940 cm−1 (out-of-plane carboxyl C–O–H bend). DRIFT provides the maximum number of bands and is capable of measuring hydrogen-bonded bands and CHx groups. ATR provides the good sensitivity for water and C–H/C–C bands in the range 2000–400 cm−1. FTIR–PAS reveals less bands than DRIFT but more intense bands than ATR–FTIR and shows the maximum sensitivity for absorption bands that do not appear in ATR-IR spectra and are expedient for supporting either DRIFT or FTIR–PAS along with depth-profiling. Thus, all three modalities are required for the full characterization of nanodiamonds surface functional groups." @default.
- W3109625971 created "2020-12-07" @default.
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- W3109625971 date "2020-12-13" @default.
- W3109625971 modified "2023-10-09" @default.
- W3109625971 title "Detonation Nanodiamonds: A Comparison Study by Photoacoustic, Diffuse Reflectance, and Attenuated Total Reflection FTIR Spectroscopies" @default.
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- W3109625971 doi "https://doi.org/10.3390/nano10122501" @default.
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