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- W3109898259 abstract "The optimization of electro-organic reactions poses a challenge due to the various parameters involved. Quite often those parameters are not independent from each other, leading the experimental scientist using linear approaches into an optimization loophole. We report a strategy for the optimization of the anodic oxidative dehydrogenative C,C cross-coupling reactions for the synthesis of biphenols based on Design of Experiments (DoE), which overcomes the drawbacks of linear optimization approaches. Using a fractional design, we increased the yield of a long-time investigated example reaction from 44% up to 85% and point out different suitable reaction conditions through to linear regression of the parameter space investigated." @default.
- W3109898259 created "2020-12-07" @default.
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- W3109898259 date "2021-02-01" @default.
- W3109898259 modified "2023-10-18" @default.
- W3109898259 title "Get into flow: Design of experiments as a key technique in the optimization of anodic dehydrogenative C,C cross-coupling reaction of phenols in flow electrolyzers" @default.
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- W3109898259 doi "https://doi.org/10.1016/j.electacta.2020.137420" @default.
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