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• W3111261645 endingPage "108407" @default.
• W3111261645 startingPage "108407" @default.
• W3111261645 abstract "A novel sandwiched-type vanadoselenite with the formula of K 6 H 8 [(SeV 10 O 28 (SeO 3 ) 3 ) 2 (Ni(H 2 O) 4 )]·24H 2 O has been synthesized in aqueous medium and well characterized. Experimental results demonstrated that it serving as a heterogeneous catalyst performed effectively catalytic activities toward sulfoxidation of thioethers under very mild condition. • Sandwiched vanadoselenite Se 8 V 20 Ni based on trivacant Keggin {Se 4 V 10 } building blocks. • Se 8 V 20 Ni has been characterized by IR, XPRD, TG, XPS and elemental analysis. • Se 8 V 20 Ni was exploited as heterogeneous catalysts for sulfoxidation of sulfides. A novel sandwiched-type vanadoselenite with the formula of K 6 H 8 [(SeV 10 O 28 (SeO 3 ) 3 ) 2 (Ni(H 2 O) 4 )]·24H 2 O ( 1 ) has been synthesized in aqueous medium and well characterized. Single crystal X-ray diffraction indicates that the sandwiched polyanion [(SeV 10 O 28 (SeO 3 ) 3 ) 2 (Ni(H 2 O) 4 )] 14− consisted of two trivicant Keggin building units [SeV 10 O 28 (SeO 3 ) 3 ] 8− and one interconnected Ni 2+ ion. Experimental results demonstrated that it could serve as a heterogeneous catalyst for sulfoxidation of thioethers and performed effectively catalytic activity. Under the optimized reaction condition, methyl phenyl sulfoxide could be oxidized to methyl phenyl sulfones within 1 h by using 1 mmol of the substrate, 3 mmol of TBHP and 2 μmol of the catalyst 1 at 25 °C in methanol. Moreover, catalyst 1 can also be easily recycled and reused four times without obvious decrease of catalytic activity." @default.
• W3111261645 created "2020-12-21" @default.
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• W3111261645 date "2021-02-01" @default.
• W3111261645 modified "2023-10-18" @default.
• W3111261645 title "Synthesis, structure and catalytic study of a new sandwiched-type vanadoselenite" @default.
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• W3111261645 doi "https://doi.org/10.1016/j.inoche.2020.108407" @default.
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