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- W3112463403 abstract "Abstract A continuous ceramic coating of 8 μm thick on Zr 1Nb alloy was fabricated by plasma electrolytic oxidation (PEO) in alkaline phosphate electrolyte. The high-temperature steam oxidation behavior of bare and PEO coated Zr 1Nb alloys was evaluated using a thermogravimetric analyzer (TGA) in 900–1200 °C water vapor environment. Their morphologies, compositions, phase constituents before and after the steam oxidation were characterized by scanning electron microscopy (SEM), glow discharge optical emission spectroscopy (GDOES) and X-ray diffraction (XRD). It was found that the mass gain of PEO coated Zr alloy was about 38%, 56%, 93% and 100% of bare Zr alloy after 3600 s steam oxidation at 900 °C, 1000 °C, 1100 °C and 1200 °C, respectively. The steam oxidation resistance of Zr 1Nb alloy was obviously improved after PEO treatment below 1000 °C, but was hardly enhanced above 1100 °C. The mass gain rate for Zr 1Nb alloy samples in high-temperature steam is related to the oxygen diffusion coefficients in β-Zr, α-Zr(O) and ZrO2 phases. After steam oxidation at 900–1200 °C, the oxide layers for bare and PEO coated Zr 1Nb alloys contain monoclinic zirconia (M-ZrO2) and a little tetragonal zirconia (T-ZrO2) phases below 1100 °C, but the T-ZrO2 phase disappears at 1200 °C." @default.
- W3112463403 created "2020-12-21" @default.
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- W3112463403 date "2021-02-01" @default.
- W3112463403 modified "2023-10-17" @default.
- W3112463403 title "High temperature oxidation of Zr 1Nb alloy with plasma electrolytic oxidation coating in 900–1200 °C steam environment" @default.
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- W3112463403 doi "https://doi.org/10.1016/j.surfcoat.2020.126768" @default.
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