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- W3113643573 abstract "Herein, a new 2-dimensional coordination polymer based on copper (II), {Cu2(L)(DMF)2}n, where L stands for 1,2,4,5-benzenetetracarboxylate (complex 1) is synthesized. Interestingly, we demonstrate that both solvent and sonication are relevant in the top-down fabrication of nanostructures. Water molecules are intercalated in suspended crystals of complex 1 modifying not only the coordination sphere of Cu(II) ions but also the final chemical formula and crystalline structure obtaining {[Cu(L)(H2O)3]·H2O}n (complex 2). On the other hand, ultrasound is required to induce the nanostructuration. Remarkably, different morphologies are obtained using different solvents and interconversion from one morphology to another seems to occur upon solvent exchange. Both complexes 1 and 2, as well as the corresponding nanostructures, have been fully characterized by different means such as infrared spectroscopy, x-ray diffraction and microscopy." @default.
- W3113643573 created "2021-01-05" @default.
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- W3113643573 date "2021-04-01" @default.
- W3113643573 modified "2023-10-17" @default.
- W3113643573 title "Solvent-tuned ultrasonic synthesis of 2D coordination polymer nanostructures and flakes" @default.
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- W3113643573 doi "https://doi.org/10.1016/j.ultsonch.2020.105425" @default.
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