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• W3115298845 endingPage "116581" @default.
• W3115298845 startingPage "116581" @default.
• W3115298845 abstract "Polycrystalline CuMo1−xWxO4 solid solutions were studied by resonant X-ray emission spectroscopy (RXES) at the W L3-edge to follow a variation of the tungsten local atomic and electronic structures across thermochromic phase transition as a function of sample composition and temperature. The experimental results were interpreted using ab initio calculations. The crystal-field splitting parameter Δ for the 5d(W)-states was obtained from the analysis of the RXES plane and was used to evaluate the coordination of tungsten atoms. Temperature-dependent RXES measurements were successfully employed to determine the hysteretic behaviour of the structural phase transition between the α and γ phases in CuMo1−xWxO4 solid solutions on cooling and heating, even at low (x<0.10) tungsten content. It was found that tungsten ions have octahedral coordination for x>0.15 in the whole studied temperature range (90-420 K), whereas their coordination changes from tetrahedral to octahedral upon cooling for smaller (x≤0.15) tungsten content. Nevertheless, some amount of tungsten ions was found to co-exists in the octahedral environment at room temperature for x<0.15. The obtained results correlate well with the color change in these solid solutions." @default.
• W3115298845 created "2021-01-05" @default.
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• W3115298845 date "2021-02-01" @default.
• W3115298845 modified "2023-10-18" @default.
• W3115298845 title "Study of the thermochromic phase transition in CuMo<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML altimg=si3.svg><mml:msub><mml:mrow /><mml:mrow><mml:mn>1</mml:mn><mml:mo>−</mml:mo><mml:mi>x</mml:mi></mml:mrow></mml:msub></mml:math>W<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML altimg=si4.svg><mml:msub><mml:mrow /><mml:mi>x</mml:mi></mml:msub></mml:math>O<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML altimg=si5.svg><mml:msub><mml:mrow /><mml:mn>4</mml:mn></…" @default.
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• W3115298845 doi "https://doi.org/10.1016/j.actamat.2020.116581" @default.
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