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- W3115375214 abstract "Combustion synthesis is a novel technique that utilizes the exothermic heat of a chemical reaction to maintain the reaction and to rapidly prepare materials. But, hitherto, none of unified criterion for the validation of combustion synthesis has been proposed. Herein, we proposed the conditions need to be met. In terms of kinetics, at the adiabatic temperature (Tad), the diffusion distance of atoms (lTad) within 0.1 s should be larger than the particle size of the reactants(d), that is, lTad≥d. For systems that satisfy Tad/Tm,L≥1(where Tm,L is the melting point of the low-melting point component of the reactants), the presence of a liquid phase significantly increases the atomic diffusion distance from nanometers to tens of microns, making the criterion lTad≥d simplified to Tad/Tm,L≥1 in most situations. In terms of thermodynamics, the system needs to ensure that the reaction components are in an activated state, that is, Tad/Tm,H ≥0.7, where Tm,H is the melting point of the high-melting point component. The criteria for the SHS reactions proposed in this study further improve the theoretical understanding of SHS reactions, and provide guidance for exploring the ultra-fast synthesis of binary and multicomponent compounds." @default.
- W3115375214 created "2021-01-05" @default.
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- W3115375214 date "2021-04-01" @default.
- W3115375214 modified "2023-09-30" @default.
- W3115375214 title "New criteria for the applicability of combustion synthesis: The investigation of thermodynamic and kinetic processes for binary Chemical Reactions" @default.
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- W3115375214 doi "https://doi.org/10.1016/j.jallcom.2020.158465" @default.
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