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- W3117462912 abstract "Two efficient synthetic methods for preparation of 3-(trifluoromethyl)cyclobutane-1-carboxylic acid are reported starting from readily available 4-oxocyclobutane precursors. These cyclobutanones can be converted to their CF3 carbinols upon treatment with TMSCF3 and a fluoride source. The bis-carboxylate system 9 was deoxygenated by treatment of Bu3SnH and provided desired compound 1 upon decarboxylation. In the monocarboxylate system 15, the triflate could be efficiently eliminated; subsequent hydrogenation afforded cis-1." @default.
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- W3117462912 date "2020-12-21" @default.
- W3117462912 modified "2023-09-27" @default.
- W3117462912 title "Two Scalable Syntheses of 3-(Trifluoromethyl)cyclobutane-1-carboxylic Acid" @default.
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- W3117462912 doi "https://doi.org/10.1021/acs.oprd.0c00422" @default.
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