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• W3118505984 abstract "Direct asymmetric reductive amination represents an efficient means of converting ketones to α-chiral primary amines, but reported examples are very limited. We describe the development of two sets of Ru-catalyzed conditions for the direct conversion of an aryl methyl ketone to a pharmaceutically relevant chiral primary amine. In the presence of NH3, NH4Cl, and H2, a readily available dtbm-Segphos ruthenium catalyst can be used to prepare the desired chiral primary amine with >93% ee on multikilogram scale." @default.
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• W3118505984 date "2021-01-12" @default.
• W3118505984 modified "2023-09-26" @default.
• W3118505984 title "Development and Scale-Up of a Direct Asymmetric Reductive Amination with Ammonia" @default.
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• W3118505984 doi "https://doi.org/10.1021/acs.oprd.0c00522" @default.
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