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- W3118550007 abstract "• It was carried out under sunlight irradiation in aqueous. • Avoiding the usage of any metal salts in the whole procedure. • Could be applied for the synthesis of active amide quinoxalines. • The reaction could also be performed on a gram scale. • Only under irradiation of sunlight for 2.5 h. A novel visible-light-promoted N -acylation for the synthesis of amides from easily available carboxylic acids with amines in the presence of I 2 within 2.5 h in aqueous solution has been developed. Using sunlight as the visible light source greatly reduces the cost of experiments and produces almost no toxic effects. Hence, this study provides an alternative catalytic system for the construction of a wide range of amides with readily available materials. Moreover, the strategy was successfully applied in the preparation of N -(3-(2,6-dimethoxyphenoxy)-7-nitroquinoxalin-2-yl)benzohydrazide, which displayed a signification anti-proliferation effect on A549, MCF-7 and HCT116 cell lines." @default.
- W3118550007 created "2021-01-18" @default.
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- W3118550007 date "2021-02-01" @default.
- W3118550007 modified "2023-10-13" @default.
- W3118550007 title "Visible-light-induced direct construction of amide bond from carboxylic acids with amines in aqueous solution" @default.
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- W3118550007 doi "https://doi.org/10.1016/j.tetlet.2020.152801" @default.
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