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- W3118644194 abstract "In this study, three fascinating resorcin[4]arene‐based Cu(I) complexes, named [CuCl (TPC4R)] ( 1 ), [CuBr (TPC4R)] ( 2 ), and [Cu 2 I 2 (TPC4R)] ( 3 ) were prepared by using a pyrimidine‐functionalized resorcin[4]arene ligand (TPC4R). In 1 and 2 , two Cu(I) ions were linked by two TPC4R and two Cl − (or Br − ) anions to form binuclear units. The adjacent units were extended into supramolecular layers through H bonds. In 3 , two Cu(I) ions were connected by one TPC4R and two I − anions to form a mononuclear complex. The mononuclear units were connected by hydrogen bonds to produce a supramolecular chain. Significantly, 1 and 2 exhibit high efficiency and universality for azide‐alkyne cycloaddition reactions in the synthesis 1,2,3‐triazoles and β ‐OH‐1,2,3‐triazoles. It has been found that the amount of catalyst, solvent type and reaction temperature have considerable influences on the activities of catalytic systems. The conversions of catalysts 1 and 2 could reach 99% for most of the selected substrates. It was found that after repeatedly used for 4 times, the catalytic activity of 1 did not decrease apparently." @default.
- W3118644194 created "2021-01-18" @default.
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- W3118644194 date "2021-01-06" @default.
- W3118644194 modified "2023-09-23" @default.
- W3118644194 title "Resorcin[4]arene‐based Cu(I) binuclear and mononuclear complexes as efficient catalysts for azide‐alkyne cycloaddition reactions" @default.
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- W3118644194 doi "https://doi.org/10.1002/aoc.6146" @default.
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