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- W3119921288 abstract "The first total syntheses of punicafolin (1) and macaranganin (2) were achieved in seven steps, respectively, from commercial α-d-glucose. The characteristic features of the synthesis are (1) sequential site-selective introduction of the adequate galloyl groups into unprotected d-glucose by a catalyst-controlled manner and (2) stereodivergent construction of the 3,6-HHDP bridge by oxidative phenol coupling of a common intermediate via a ring-flipping process of the glucose core. Because no protective groups were used for glucose throughout the process, extremely short-step total syntheses of natural glycosides 1 and 2 (MW 938) were performed." @default.
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- W3119921288 date "2021-01-14" @default.
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- W3119921288 title "Seven-Step Stereodivergent Total Syntheses of Punicafolin and Macaranganin" @default.
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- W3119921288 doi "https://doi.org/10.1021/jacs.0c10714" @default.
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