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• W3120285943 abstract "The cleavage of benzyl ethers by catalytic hydrogenolysis or Birch reduction suffers from poor functional group compatibility and limits their use as a protecting group. The visible-light-mediated debenzylation disclosed here renders benzyl ethers temporary protective groups, enabling new orthogonal protection strategies. Using 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) as a stoichiometric or catalytic photooxidant, benzyl ethers can be cleaved in the presence of azides, alkenes, and alkynes. The reaction time can be reduced from hours to minutes in continuous flow." @default.
• W3120285943 created "2021-01-18" @default.
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• W3120285943 date "2021-01-05" @default.
• W3120285943 modified "2023-10-14" @default.
• W3120285943 title "Visible-Light-Mediated Oxidative Debenzylation Enables the Use of Benzyl Ethers as Temporary Protecting Groups" @default.
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• W3120285943 doi "https://doi.org/10.1021/acs.orglett.0c04026" @default.
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