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• W3120331389 abstract "A straightforward method for the undirected trifluoromethylation of unactivated methylene units was developed. The reaction proceeds in aqueous acetonitrile with Grushin's reagent, bpyCu(CF3)3, under broad-spectrum white-light irradiation. The trifluoromethylation tolerates a wide range of functional groups including ketones, esters, nitriles, amides, alcohols, and carboxylic acids. The C-H cleavage step is performed via intermolecular H atom abstraction, and the selectivities across a range of methylene units are reported. Mechanistic studies offer a general reaction coordinate for the overall transformation." @default.
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• W3120331389 date "2021-01-14" @default.
• W3120331389 modified "2023-10-14" @default.
• W3120331389 title "Csp³–H Trifluoromethylation of Unactivated Aliphatic Systems" @default.
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• W3120331389 doi "https://doi.org/10.1021/acs.orglett.0c03891" @default.
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