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• W3122062030 abstract "The square-planar nickel(II) title complex, [Ni(C 24 H 36 F 2 N 6 )](ClO 4 ) 2 or [Ni L ](ClO 4 ) 2 ( L = 3,10-bis(4-fluorophenethyl)-1,3,5,8,10,12-hexaazacyclotetradecane) was synthesized by a one-pot reaction of template condensation and its X-ray crystal structure was determined. The nickel(II) ion lies close by a twofold axis and the complex displays whole-molecule disorder. Ligand L , a hexaazacyclotetradecane ring having 4-fluorophenethyl side chains attached to uncoordinated nitrogen atoms, adopts a trans III ( R,R,S , S) configuration. The average Ni—N bond distance is 1.934 (9) Å, which is quite similar to those of other nickel(II) complexes with similar ligands. The nickel(II) ion is located 0.051 (7) Å above the least-squares plane through the four coordinated N atoms. The average C—N bond distance and C—N—C angle involving uncoordinated nitrogen atoms are 1.425 (12) Å and 118.0 (9)°, respectively, indicating a significant contribution of sp 2 hybridization for these N atoms. The intermolecular N—H...O, C—H...O/F hydrogen bonds of the complex form a network structure, which looks like a seamless floral lace pattern." @default.
• W3122062030 created "2021-02-01" @default.
• W3122062030 creator A5024595159 @default.
• W3122062030 creator A5086570283 @default.
• W3122062030 date "2021-01-22" @default.
• W3122062030 modified "2023-10-17" @default.
• W3122062030 title "Crystal structure of [3,10-bis(4-fluorophenethyl)-1,3,5,8,10,12-hexaazacyclotetradecane]nickel(II) diperchlorate" @default.
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• W3122062030 doi "https://doi.org/10.1107/s2056989020016795" @default.
• W3122062030 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/7869553" @default.
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