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- W3122374073 abstract "Heterophase TiO2 nanoparticles formed in the presence of a very low concentration of a substance with two donor groups were studied and the mechanism of their formation was proposed. The TiO2 nanoparticles were prepared by low-temperature hydrolysis and polycondensation of Ti (IV) n-propoxide in the presence of lactic acid (LA). The phase composition of the nanoparticles was controlled by the LA/Ti molar ratio ranging from 0.02 to 3.0. At low LA/Ti molar ratios, biphasic anatase-brookite was formed, at average LA/Ti molar ratios, anatase-brookite-rutile particles were formed, and at high molar ratios, pure anatase was formed. By using the low LA/Ti molar ratios, the low-temperature colloidal synthesis made it possible to control the composition of heterophase mesoporous TiO2 nanoparticles with a high specific surface area and high photocatalytic activity in the production of hydrogen by water splitting. The highest photocatalytic activity was exhibited by anatase-brookite nanoparticles containing 46–65% brookite, synthesized at LA/Ti molar ratios in the range of 0. 033 to 0.1." @default.
- W3122374073 created "2021-02-01" @default.
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- W3122374073 date "2021-02-01" @default.
- W3122374073 modified "2023-10-16" @default.
- W3122374073 title "Influence of LA/Ti molar ratio on the complex synthesis of anatase/brookite nanoparticles and their hydrogen production" @default.
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- W3122374073 doi "https://doi.org/10.1016/j.ijhydene.2020.12.080" @default.
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