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- W3123129871 abstract "This work investigated the spark plasma sintering behavior of mechanochemically synthesized molybdenum silicide (MS) powders. Nanosized MS powders were obtained via a mechanochemical synthesis process applied to the initial MoO3–SiO2–Mg powder batches. Various characterization techniques such as X-ray diffraction (XRD), particle size analysis (PSA), Fourier-transform infrared spectroscopy (FTIR), and transmission electron microscopy (TEM) were performed to reveal the compositional and morphological properties of the homemade MS powders. The increasing sintering temperature up to 1600 °C enhanced the sinterability of the MS samples. In addition to the XRD and SEM/EDS analyses, the samples sintered at different temperatures were also characterized in terms of Archimedes' density, microhardness, and fracture toughness properties. The MS sample sintered at the temperature of 1600 °C demonstrated a relative density of 93.7%, a Vickers microhardness of 14.9 GPa, and a fracture toughness of 3.54 MPa√m. The wear rate decreased significantly with increasing sintering temperature from 3.60 × 10−5 mm3/Nm (1500 °C) to 1.77 × 10−5 mm3/Nm (1600 °C). Lastly, thermal gravimetry analyses (TGA) were conducted to observe the oxidation behavior of the sintered samples. The oxidation resistance of MS samples improved with increasing sintering temperatures." @default.
- W3123129871 created "2021-02-01" @default.
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- W3123129871 date "2021-05-01" @default.
- W3123129871 modified "2023-10-03" @default.
- W3123129871 title "Spark plasma sintering of molybdenum silicides synthesized from oxide precursors" @default.
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- W3123129871 doi "https://doi.org/10.1016/j.ceramint.2021.01.248" @default.
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