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• W3124454989 endingPage "2865" @default.
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• W3124454989 abstract "We describe, for the first time, two protocols for direct difluoromethylation of unactivated alkyl bromides and iodides. Reactions of alkyl iodides with TMSCF2H were mediated by a copper catalyst using CsF as the activator, while reactions of less reactive alkyl bromides required a combination of palladium and a stoichiometric amount of CuI as the catalysts. Preliminary mechanistic studies of the synergistic Pd/Cu-catalyzed difluoromethylation of alkyl bromides suggest that it proceeds likely via a Pd(I)/Pd(III) catalytic cycle." @default.
• W3124454989 created "2021-02-01" @default.
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• W3124454989 date "2021-01-19" @default.
• W3124454989 modified "2023-09-29" @default.
• W3124454989 title "Difluoromethylation of Alkyl Bromides and Iodides with TMSCF₂H" @default.
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• W3124454989 doi "https://doi.org/10.1021/acs.joc.0c02783" @default.
• W3124454989 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/33464896" @default.
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