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- W3124698522 abstract "Modified procedure for the synthesis of atropine (1) has been achieved. The synthetic approach commenced with a modified Robinson-Schopf reacton. The condensation of 2, 5-dimethoxytetrahydrofuran (9), methylamine hydrochloride, and acetonedicarboxylic acid (8) afforded tropinone (4). Catalytic hydrogenation of compound 4 stereoselectively produced tropine (2). Esterification of tropic acid (3) and tropine (2) gave atropine (1) Atropine sulfate (10) was obtained by adding dilute sulfuric acid solution in acetone to atropine (1) followed by recrystallization." @default.
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- W3124698522 date "1982-03-01" @default.
- W3124698522 modified "2023-09-23" @default.
- W3124698522 title "A Modified Synthesis of Atropine" @default.
- W3124698522 doi "https://doi.org/10.6522/bicas.1982.29.2" @default.
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