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- W3125477770 abstract "Reactions of [PhC(NtBu)2]ECl (E = Si, Ge) with Li[(3,5-Me2-C6H3)NPiPr2] afforded the mixed donor ligands [PhC(NtBu)2]E[(3,5-Me2-C6H3)NPiPr2] (1, E = Si; 2, E = Ge) in high yields. Further reaction of these ligands 1 and 2 with the complex Ni(cod)2 readily generated their corresponding phosphine-functionalized silylene or germylene nickel(0) complexes 3 and 4, respectively. Treatment of these complexes 3 and 4 with Ad–C≡P afforded 1,3-diphosphacyclobutadiene complexes 5 and 6, respectively, via selective head-to-tail cyclization of two phosphaalkynes. The reaction of 4 with 2,4,6-tri-tert-butyl-1-nitrosobenzene (Ar*NO) formed complex 7 as the first example of a mixed donor ligand stabilized Ni nitrosoarene complex." @default.
- W3125477770 created "2021-02-01" @default.
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- W3125477770 date "2021-01-17" @default.
- W3125477770 modified "2023-09-30" @default.
- W3125477770 title "Synthesis and Reactivity of Side-Arm Phosphine Functionalized Amidinatosilylene- and Amidinatogermylene-Supported Nickel(0) Complexes" @default.
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- W3125477770 doi "https://doi.org/10.1021/acs.organomet.0c00770" @default.
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