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- W3126799255 abstract "Herein, we report the solvent-free synthesis of ZSM-5 zeolites assisted by the small organic lactam. i.e., N-methyl-2-pyrrolidone (NMP). An array of characterization techniques (XRD, FTIR, and SEM) confirmed the formation of intergrown, highly crystalline ZSM-5 with a size of around 10 μm. To investigate the structure of NMP within the ZSM-5 synthesis, we have performed the 13C liquid NMR spectroscopy measurement, which showed the presence of preserved NMP (cyclic molecule) and a ring-opened NMP molecule. Ultimately, a density functional theory (DFT)-based computational study resulted in the negative formation energies suggested that both molecules could be stabilized within the straight and zig-zag channels of ZSM-5 frameworks. To the best of our knowledge, this is the first time NMP can be utilized as an organic structure-directing agent for crystallizing ZSM-5 zeolites." @default.
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- W3126799255 date "2021-05-01" @default.
- W3126799255 modified "2023-10-01" @default.
- W3126799255 title "Solvent-free, small organic lactam-assisted synthesis of ZSM-5 zeolites" @default.
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- W3126799255 doi "https://doi.org/10.1016/j.matlet.2021.129501" @default.
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