Matches in SemOpenAlex for { <https://semopenalex.org/work/W3129538410> ?p ?o ?g. }
Showing items 1 to 54 of
54
with 100 items per page.
- W3129538410 endingPage "6" @default.
- W3129538410 startingPage "2213" @default.
- W3129538410 abstract "In the study, N-tert-butylbenzothiazole-2-sulphenamide (TBBS) was synthesized with one-step method with hydrogen peroxide as the oxidant. TBBS was detected and characterized with FTIR，UV-Vis，XRD and TG-DSC. Its micro-structure and intrinsic regularity were revealed. Chemical bond types into TBBS molecule were revealed with FTIR. The final product was determined TBBS. Three absorption peaks were detected by UV-Vis at 228.3，281.5，298.3 nm respectively, due to n→σ*，π→π*，n→π* electronic transitions. It could provide experimental basis with enterprise to test TBBS product quality and speculate its structure. The phase composition and structure of TBBS were revealed by crystallographic data from XRD detecting such as cell parameters, crystal face index. The phase composition and qualitative identification of TBBS structure were completed. Two kinds of information were detected by TG-DSC as quality change and thermal effect. The DSC curve of TBBS was very complex. There were a small absorption peak of 53.3 ℃ as a small amount of tert-butylamine containing in TBBS was oxidized. Three exothermic peaks of 117.4，269.2，373.7 ℃, due to transition peak and decomposition phase of TBBS respectively. The decomposition temperature of TBBS was very high. It could provide reference for research on rubber vulcanizing properties by TBBS on rubber vulcanizing machine. This study could provide the basis experimental data on the enterprises to designate the working standard tracing detection of TBBS industrialized production. The performance index of TBBS was judged. The project of TBBS industry standard could be declared by the enterprises, written a draft standard." @default.
- W3129538410 created "2021-03-01" @default.
- W3129538410 creator A5007070288 @default.
- W3129538410 creator A5021376590 @default.
- W3129538410 creator A5031924033 @default.
- W3129538410 creator A5048797612 @default.
- W3129538410 creator A5058662433 @default.
- W3129538410 creator A5060286180 @default.
- W3129538410 date "2016-07-01" @default.
- W3129538410 modified "2023-09-26" @default.
- W3129538410 title "[Study on the Preparation of N-Tert-Butylbenzothiazole-2-Sulphenamide and Its Spectral Analysis]." @default.
- W3129538410 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/30035991" @default.
- W3129538410 hasPublicationYear "2016" @default.
- W3129538410 type Work @default.
- W3129538410 sameAs 3129538410 @default.
- W3129538410 citedByCount "0" @default.
- W3129538410 crossrefType "journal-article" @default.
- W3129538410 hasAuthorship W3129538410A5007070288 @default.
- W3129538410 hasAuthorship W3129538410A5021376590 @default.
- W3129538410 hasAuthorship W3129538410A5031924033 @default.
- W3129538410 hasAuthorship W3129538410A5048797612 @default.
- W3129538410 hasAuthorship W3129538410A5058662433 @default.
- W3129538410 hasAuthorship W3129538410A5060286180 @default.
- W3129538410 hasConcept C113196181 @default.
- W3129538410 hasConcept C124681953 @default.
- W3129538410 hasConcept C178790620 @default.
- W3129538410 hasConcept C185592680 @default.
- W3129538410 hasConcept C43617362 @default.
- W3129538410 hasConceptScore W3129538410C113196181 @default.
- W3129538410 hasConceptScore W3129538410C124681953 @default.
- W3129538410 hasConceptScore W3129538410C178790620 @default.
- W3129538410 hasConceptScore W3129538410C185592680 @default.
- W3129538410 hasConceptScore W3129538410C43617362 @default.
- W3129538410 hasIssue "7" @default.
- W3129538410 hasLocation W31295384101 @default.
- W3129538410 hasOpenAccess W3129538410 @default.
- W3129538410 hasPrimaryLocation W31295384101 @default.
- W3129538410 hasRelatedWork W1979022052 @default.
- W3129538410 hasRelatedWork W1981041592 @default.
- W3129538410 hasRelatedWork W2082740623 @default.
- W3129538410 hasRelatedWork W2136570285 @default.
- W3129538410 hasRelatedWork W2313486456 @default.
- W3129538410 hasRelatedWork W2314834460 @default.
- W3129538410 hasRelatedWork W2320126264 @default.
- W3129538410 hasRelatedWork W2331094303 @default.
- W3129538410 hasRelatedWork W2950162563 @default.
- W3129538410 hasRelatedWork W3005337525 @default.
- W3129538410 hasVolume "36" @default.
- W3129538410 isParatext "false" @default.
- W3129538410 isRetracted "false" @default.
- W3129538410 magId "3129538410" @default.
- W3129538410 workType "article" @default.