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- W3131036488 abstract "The direct β-functionalization of saturated aza-heterocycles has remained a synthetic challenge because of the remote and unactivated nature of β-C-H bonds in these motifs. Herein, we demonstrate the β-functionalization of saturated aza-heterocycles enabled by a two-step organic photoredox catalysis approach. Initially, a photoredox-catalyzed copper-mediated dehydrogenation of saturated aza-heterocycles produces ene-carbamates. This is followed by an anti-Markovnikov hydrofunctionalization of the ene-carbamates with a range of heteroatom-containing nucleophiles furnishing an array of C-C, C-O, and C-N aza-heterocycles at the β-position." @default.
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- W3131036488 date "2021-02-24" @default.
- W3131036488 modified "2023-10-11" @default.
- W3131036488 title "β-Functionalization of Saturated Aza-Heterocycles Enabled by Organic Photoredox Catalysis" @default.
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- W3131036488 doi "https://doi.org/10.1021/acscatal.1c00099" @default.
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