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- W3133287070 abstract "In this work, the synthesis of hydrous zirconia by controlled double-jet precipitation (CDJP) was carried out in the pH range from 3 to 8. The evolution of particle shape and size during precipitation was investigated. It was found that at pH 3, 7, and 8 during the precipitation process there is no significant change in particle size, the suspension was gel-like, particles actively aggregated during drying. A gradual increase in particle size and a decrease in particle size dispersion specific for layer-by-layer aggregation was observed during CDJP at pH 4 to 6. The resulting particles do not aggregate and retain a rounded globular shape with a narrow size distribution during drying. Samples obtained at a pH above 6 are characterized after drying by a high specific surface area and porosity, as well as a reduced content of NO3- ions. The effect of pH precipitation on the phase composition and crystallite size of calcined samples was discussed." @default.
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- W3133287070 date "2021-05-01" @default.
- W3133287070 modified "2023-09-24" @default.
- W3133287070 title "A new approach for the synthesis of monodisperse zirconia powders with controlled particle size" @default.
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- W3133287070 doi "https://doi.org/10.1016/j.ijhydene.2021.01.134" @default.
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