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- W3133622467 endingPage "132055" @default.
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- W3133622467 abstract "Most of the previous syntheses of the marine natural product 6-bromotryptamine have almost certainly led to partial debromination resulting in an impure product containing tryptamine. We show that loss of bromine occurs when lithium aluminum hydride is employed as a reducing agent in the final reaction step leading to 6-bromotryptamine. Reductive-debromination is also likely to intrude during some of the syntheses of 6-bromoindole, the typical precursor to 6-bromotryptamine. None of the seven described syntheses of 6-bromotryptamine that involve a reduction sequence from 6-bromoindole have reported elemental analyses as a measure of purity." @default.
- W3133622467 created "2021-03-15" @default.
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- W3133622467 date "2021-04-01" @default.
- W3133622467 modified "2023-09-25" @default.
- W3133622467 title "Concerning the preparation of 6-bromotryptamine" @default.
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- W3133622467 doi "https://doi.org/10.1016/j.tet.2021.132055" @default.
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