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- W3133759892 abstract "(1 – x)PbVO3–xBiCoO3 solid solutions with 0 ≤ x ≤ 1 were prepared at a high pressure of 5–6 GPa and a high temperature of 1223–1473 K. They adopt a polar tetragonal P4mm structure for the 0 ≤ x ≤ 0.3 and 0.75 ≤ x ≤ 1 ranges with giant tetragonal distortions and a cubic Pm3̅m structure for the 0.4 ≤ x ≤ 0.7 range. High-temperature structural studies with synchrotron X-ray powder diffraction showed that polarization, calculated by the point-charge model, and the tetragonal distortion remained nearly constant in the x = 0.8 sample from 295 K up to the decomposition temperature of about 700 K. Magnetic and differential scanning calorimetry measurements showed that the Néel temperature, TN, nearly linearly decreased from 470 K for x = 1 to 250 K for x = 0.75 (with TN = 395 K for x = 0.9 and TN = 295 K for x = 0.8). Long-range magnetic ordering also takes place at TN = 44 K for x = 0. All other samples with 0.1 ≤ x ≤ 0.7 demonstrated spin-glass-like magnetic properties and notably reduced Weiss temperatures. Effective magnetic moments estimated for the x = 0.6, 0.65, and 0.7 cubic samples gave evidence that cobalt is present in the +2 and +3 oxidation states, and Co3+ cations take the low-spin state." @default.
- W3133759892 created "2021-03-15" @default.
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- W3133759892 date "2021-03-08" @default.
- W3133759892 modified "2023-09-26" @default.
- W3133759892 title "Solid Solutions between PbVO<sub>3</sub> and BiCoO<sub>3</sub>" @default.
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- W3133759892 doi "https://doi.org/10.1021/acs.inorgchem.1c00030" @default.
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