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- W3134729904 abstract "We present a DSC and X-ray scattering study investigating the effect of polyhedral oligomeric silsesquioxane (POSS) block crystallinity on the self-assembly of a poly(acryloisobutyl polyhedral oligomeric silsesquioxane)-b-poly(ethylene oxide)-b-poly(acryloisobutyl polyhedral oligomeric silsesquioxane) (POSS-PEO-POSS) triblock copolymer and poly(ethylene oxide)-b- poly(acryloisobutyl polyhedral oligomeric silsesquioxane) (PEO-POSS) diblock copolymers mixed with lithium bis(trifluoromethanesulfonyl)imide salt. The POSS block in all copolymer/salt mixture organizes into a rhombohedral crystal, similar to that of the POSS homopolymer. Semicrystalline polymer/salt mixtures favor morphologies with flat interfaces (i.e., lamellae) despite the asymmetric nature of the copolymers; PEO/salt volume fractions range from 0 to 0.85. Coexisting lamellae and hexagonally packed cylinders as well as coexisting lamellae with different domain spacings are seen in many copolymer/salt mixtures wherein the POSS block is amorphous. Morphological phase transitions in these systems are seen in the vicinity of the POSS crystallization temperature." @default.
- W3134729904 created "2021-03-15" @default.
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- W3134729904 date "2021-06-01" @default.
- W3134729904 modified "2023-10-13" @default.
- W3134729904 title "Effect of crystallization of the polyhedral oligomeric silsesquioxane block on self-assembly in hybrid organic-inorganic block copolymers with salt" @default.
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- W3134729904 doi "https://doi.org/10.1016/j.giant.2021.100055" @default.
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