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• W3134985682 startingPage "1383" @default.
• W3134985682 abstract "ABSTRACT A concise synthesis of a plasmenylethanolamine (PlsEtn-[16:0/18:1 n-9]), known as antioxidative phospholipids commonly found in cell membranes, has been achieved from an optically active known diol through 8 steps. The key transformations for the synthesis of PlsEtn-[16:0/18:1 n-9] are (1) regio- and Z-selective vinyl ether formation via the alkylation of a lithioalkoxy allyl intermediate with an alkyl iodide, and (2) a one-pot phosphite esterification–oxidation sequence to construct the ethanolamine phosphonate moiety in the presence of the vinyl ether functionality. The piperidine salt of synthetic PlsEtn-[16:0/18:1 n-9] was desalinated through reversed-phase high-performance liquid chromatography purification." @default.
• W3134985682 created "2021-03-15" @default.
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• W3134985682 date "2021-03-11" @default.
• W3134985682 modified "2023-10-03" @default.
• W3134985682 title "Synthesis of a plasmenylethanolamine" @default.
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• W3134985682 doi "https://doi.org/10.1093/bbb/zbab037" @default.
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• W3134985682 hasPublicationYear "2021" @default.
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