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• W3136620004 endingPage "6417" @default.
• W3136620004 startingPage "6401" @default.
• W3136620004 abstract "Microwave-assisted heating methods have been used to synthesize oleylamine-capped Ge1–xSnx nanocrystals. By varying the reaction temperature while keeping the Ge and Sn precursor concentrations constant, Ge1–xSnx nanocrystals with Sn compositions of 13.9 ± 2.1% over the 3.8–9.3 nm size range have been achieved. The oleylamine-capping ligand is replaced with dodecanethiol without affecting the Sn composition of the nanocrystals. The Sn composition is obtained from employing Vegard’s law on the lattice parameters obtained from the Rietveld refinement of powder X-ray diffraction patterns. Scanning transmission electron microscopy provides particle size and morphology. Extended X-ray absorption fine structure at the Sn and Ge edges of the dodecanethiol-capped nanocrystals confirms the solid solution, which is further supported by Raman spectroscopy. 1H NMR and FTIR are used to characterize the surface ligand capping before and after ligand exchange. Tauc plot analysis of UV–vis–NIR spectra to determine the indirect optical band gap for oleylamine- and dodecanethiol-capped Ge1–xSnx nanocrystals is reported. This work demonstrates the effects of synthesis temperature on the particle size, composition, and structure of Ge1–xSnx nanocrystals." @default.
• W3136620004 created "2021-03-29" @default.
• W3136620004 creator A5003289411 @default.
• W3136620004 creator A5020953405 @default.
• W3136620004 creator A5056081806 @default.
• W3136620004 creator A5080920602 @default.
• W3136620004 creator A5081073058 @default.
• W3136620004 date "2021-03-16" @default.
• W3136620004 modified "2023-10-16" @default.
• W3136620004 title "Structural Characterization of Oleylamine- and Dodecanethiol-Capped Ge_1–<i>x</i>Sn_<i>x</i> Alloy Nanocrystals" @default.
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