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- W3136803411 abstract "A new x-ray isothermal furnace has been developed, suitable for in situ observations of semi-solid processes including the transition from dendritic to globulitic grain morphology and grain coarsening in metallic samples. A homogeneous, isothermal temperature field is achieved using a novel heater concept. The furnace structure is sandwich-like with heating elements positioned in the beam line and parallel to the sample. Planar heat transfer to the sample enables measurements with low cooling rates and a minimized temperature gradient. Cooling rates from 0.1 to 15 K min−1 can be controlled in the temperature range 1170–670 K. The furnace setup is integrable in the existing rotatable laboratory x-ray facility (X-RISE) at the German Aerospace Center (DLR). In this setup, an effective pixel size of 3 μm and a field of view of 8 mm in diameter can be achieved. Preliminary solidification and semi-solid experiments in the hypo-eutectic alloy systems Al–Ge and Al–Cu, inoculated with Al–5Ti–1B grain refiner, are presented. They indicate a very uniform temperature distribution in the sample." @default.
- W3136803411 created "2021-03-29" @default.
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- W3136803411 date "2021-03-01" @default.
- W3136803411 modified "2023-09-27" @default.
- W3136803411 title "Isothermal furnace for long-term <i>in situ</i> and real-time X-radiography solidification experiments" @default.
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- W3136803411 doi "https://doi.org/10.1063/5.0037398" @default.
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