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• W3136943310 abstract "• Synthesis of chiral pincer ligands. • No racemization occurs upon complexation and metalation. • Chiral ligand-metal cooperating catalysts. This paper reports an efficient synthetic approach to preparing optically active PC( sp 3 )P pincer ligands and their complexes. The reported synthetic scheme relies on a simple and straightforward carbo-Diels–Alder reaction cycloaddition of a readily available phosphine precursor, 1,8-bis-(diphenylphosphino)anthracene ( 2 ) with enantiomerically pure bis -(methyl-(S)-lactyl) fumarate (3) leading to the formation of chromatographically resolvable diastereomers 4 and 4′ that can be converted into a pair of enantiomerically pure antipodes 1 and 1′ . We demonstrated that no racemization occurs upon complexation and metalation of the bifunctional PC( sp 3 )P pincer ligands." @default.
• W3136943310 created "2021-03-29" @default.
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• W3136943310 date "2021-06-01" @default.
• W3136943310 modified "2023-10-13" @default.
• W3136943310 title "Synthesis and characterization of chiral enantiopure PC(sp)P pincer ligands and their complexes" @default.
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• W3136943310 doi "https://doi.org/10.1016/j.ica.2021.120350" @default.
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