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- W3139278844 abstract "Abstract In this study, boride nanoparticles were synthesized via a low‐cost and simple pulsed discharge of compacted crystalline and amorphous B micron‐sized powders for the first time. Borides of Ti, Mo, W, and Zr were chosen for synthesis experiments. The as‐synthesized powders were spherically shaped and smaller than 100 nm. X‐ray diffraction patterns indicated the presence of several minor phases in each boride powder in addition to a single main‐phase boride. Specifically, the main phases were TiB 2 , MoB 2 , WB 4 , and ZrB 2 for borides of Ti, Mo, W, and Zr, respectively. Energy‐dispersive spectroscopy (EDS) indicated the presence of B and metal in almost all particles of every sample. The observed particles usually exhibited a two‐part structure: a boride phase and B. Small amounts of C, Fe, Cr, and Ni were detected by EDS; however, the contents of Fe, Cr, and Ni were substantially reduced after improvements to the experimental setup." @default.
- W3139278844 created "2021-03-29" @default.
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- W3139278844 date "2021-05-10" @default.
- W3139278844 modified "2023-10-17" @default.
- W3139278844 title "Nanoparticle synthesis of transition‐metal borides by pulsed discharge of compacted powder" @default.
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- W3139278844 doi "https://doi.org/10.1111/jace.17780" @default.
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