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- W3140670801 abstract "By using a flexible multidentate ligand,bis(2-hydroxyethyl)iminotris(hydroxyhydroxylmethy)methane('bis-tris':H5L),the title complex {[Na(H6L)2]2}n·nV10O28(1) has been successfully synthesized under self-assembly condition and characterized by IR spectroscopy,elemental analysis,PXRD and single-crystal X-ray diffraction.The crystal structure belongs to an orthorhombic system,space group Cmca with a = 23.752(2),b = 13.5360(8),c = 18.5377(11) ,V = 5960.1(7),Z = 8,Dc = 2.055 g/cm3,F(000) = 3744,μ = 1.630 mm-1,the final R = 0.0283 and wR = 0.0759 for 3353 observed reflections with I 2σ(I).This complex consists of decavanadate [V10O28]6-motifs as counter anions intercalated with one-dimensiond chains of the composition [Na(H6L)2]n3n+.And significant intermolecular O-H…O hydrogen-bonding interactions lead to a three-dimensional supramolecular framework." @default.
- W3140670801 created "2021-04-13" @default.
- W3140670801 creator A5076884755 @default.
- W3140670801 date "2012-01-01" @default.
- W3140670801 modified "2023-09-24" @default.
- W3140670801 title "Synthesis,Crystal Structure and Properties of a Novel Decavanadate Complex with One-dimensional Chain Involving Sodium and 'Bis-tris' Ligand" @default.
- W3140670801 hasPublicationYear "2012" @default.
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