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- W3141512954 abstract "Atomic layer deposition has been employed for postsynthesis treatment of octadecyl bonded silica ( ODS) as a typical reversed-phase stationary phase for high performance liquid chromatography( HPLC) ,in an effort to alleviate peak tailing for basic compounds. With hexamethyldisilazane( HMDS) as an endcapping agent,the ODS packing materials were heated to 250 ℃ and maintained at that temperature for 6 h,affording packing materials which are highly inert to basic compounds. Chromatographic performance in terms of reten-tion factor and tailing factor of the resulting phases was evaluated using phenol/pyridine and naphthalene/amitriptyline pairs as probes. The results were compared with those for the same packing treated by liquid phase method and for the commercial products including Zorbax SB-C18 and Kromasil C18. The separation characteristics of the ODS phase obtained by atomic layer deposition appear to be superior to that by liquid phase method and,comparable with or even better than the commercial products studied. Being solvent-free process amenable to mass production,the described method provides an economical and eco-friendly approach to manufacturing HPLC packing materials on industrial scale." @default.
- W3141512954 created "2021-04-13" @default.
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- W3141512954 date "2009-01-01" @default.
- W3141512954 modified "2023-09-25" @default.
- W3141512954 title "Endcapping of Octadecyl Bonded Silica by Atomic Layer Deposition for Separation of Basic Compounds" @default.
- W3141512954 hasPublicationYear "2009" @default.
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