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- W3141924492 abstract "Zirconium 3-nitrophthalate (Zr(3-NO2-PHT)2·2H2O) was synthesized using 3-nitrophthalic acid, sodium hydroxide, and zirconyl nitrate as raw materials. Its structure was determined by elemental analysis, X-ray fluorescence and FT-IR spectra. The thermal decomposition mechanism and kinetic parameters of the decomposition reaction for Zr(3-NO2-PHT)2·2H2O were investigated by temperature-programmed TG-DTG and condensed-phase thermolysis/FT- IR techniques. A kinetic equation for the decomposition reaction was obtained. The results showed that Zr(3-NO2-PHT)·2 2H2O underwent a four-stage decomposition process and that the main decomposition reaction occurred during the second process. The apparent activation energy (Ea) and pre-exponential factor (A) of the main decomposition reaction are 158.84 kJ·mol-1 and 109.85 s-1, respectively. The kinetic equation can thus be expressed as: dα/dt=109.85(1-α)e-1.91×104/T." @default.
- W3141924492 created "2021-04-13" @default.
- W3141924492 creator A5043630469 @default.
- W3141924492 date "2008-01-01" @default.
- W3141924492 modified "2023-09-25" @default.
- W3141924492 title "Preparation, Thermal Behavior and Non-isothermal Decomposition Reaction Kinetics of Zr(3-NO_2-PHT)_2·2H_2O" @default.
- W3141924492 hasPublicationYear "2008" @default.
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