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• W3142372854 abstract "From paints to food products, solvent evaporation is ubiquitous and critically impacts product rheological properties. It affects Newtonian fluids by concentrating any non-volatile components and viscoelastic materials, which hardens up. In both of these cases, solvent evaporation leads to a change in the sample volume, which makes any rheological measurements particularly challenging with traditional shear geometries. Here we show that the rheological properties of a sample experiencing `slow' evaporation can be monitored in a time-resolved fashion by using a zero normal-force controlled protocol in a parallel-plate geometry. Solvent evaporation from the sample leads to a decrease of the normal force, which is compensated at all times by a decrease of the gap height between the plates. As a result, the sample maintains a constant contact area with the plates despite the significant decrease of its volume. We validate the method under both oscillatory and continuous shear by accurately monitoring the viscosity of water-glycerol mixtures experiencing evaporation and a relative volume decrease as large as 70%. Moreover, we apply this protocol to dehydrating suspensions. Specifically, we monitor a dispersion of charged silica nanoparticles undergoing a glass transition induced by evaporation. While the decrease in gap height provides a direct estimate of the increasing particle volume fraction, oscillatory and continuous shear measurements allow us to monitor the suspension's evolving viscoelastic properties in real-time. Overall, our study shows that a zero normal-force protocol provides a simple approach to bulk and time-resolved rheological characterization for systems experiencing slow volume variations." @default.
• W3142372854 created "2021-04-13" @default.
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• W3142372854 date "2021-04-07" @default.
• W3142372854 modified "2023-10-12" @default.
• W3142372854 title "Time-resolved rheometry of drying liquids and suspensions" @default.
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• W3142372854 doi "https://doi.org/10.1122/8.0000214" @default.
• W3142372854 hasPublicationYear "2021" @default.
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