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- W3142507631 abstract "A gas chromatography coupled with negative chemical ionization mass spectrometric(GC-NCI-MS) method was developed for the determination of two dechlorane plus(DP) isomers in human serum sample.Target compound and serum lipid were extracted by lipid-lipid extraction.After the sulfuric acid treatment to remove extracted lipids from the samples,samples were further cleaned up with a silica/sulfuric acid column.Identification and quantification of DP were carried out by MS.The detection limit of instrument was 0.5-0.7 pg.The detection limit of the method was 15-20 pg per sample.Spiked recoveries of DP in human serum samples were in the range of 70.2%-85.7%.The developed method was further validated in human serum.DP concentrations were analyzed in 20 electronics dismantling workers and 20 reference humans,total DP concentration was 7.8-465 ng/g lipid and 0.93-50.5 ng/g lipid,respectively." @default.
- W3142507631 created "2021-04-13" @default.
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- W3142507631 date "2011-01-01" @default.
- W3142507631 modified "2023-09-27" @default.
- W3142507631 title "Quantification of Dechlorane Plus in Human Serum by Gas Chromatography Coupled with Negative Chemical Ionization Mass Spectrometry" @default.
- W3142507631 hasPublicationYear "2011" @default.
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