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• W3145159635 abstract "The stationary phase based on sol-gel ground silica monolith particles has been produced by one-pot polymerization method incorporation of styrene and ethylene dimethacrylate. First, the ground silica monolith particles were prepared by a sol-gel process followed by sedimentation. The particles were then subjected to modify with styrene ligand via one-pot polymerization, whereas ethylene dimethacrylate was used as the cross-linker. The glass lined stainless steel columns (1 mm internal diameter, 150 mm length) were packed with the above phase for estimation of the chromatographic performance in high-performance liquid chromatography. An average number of theoretical plates of as high as 39,300 plates/column was obtained under the optimized elution condition. The column-to-column reproducibility was proved satisfactory in separation efficiency and retention factor. The experimental results indicate that sol-gel ground silica particles prepared by an aid of one-pot modification can provide a better way for preparation of highly efficient stationary phase." @default.
• W3145159635 created "2021-04-13" @default.
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• W3145159635 date "2021-03-27" @default.
• W3145159635 modified "2023-10-16" @default.
• W3145159635 title "Polystyrene Immobilized Sol–Gel Ground Silica Monolith Particles Using One-Pot Reaction of Enhanced Separation Efficiency" @default.
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• W3145159635 doi "https://doi.org/10.1093/chromsci/bmab032" @default.
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