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• W3145645636 abstract "Abstract Two new aqueous U IV complexes were synthesized by the interaction between the tetravalent uranium cation and the ( 1,4,7,10‐Tetraazacyclododecane‐1,4,7,10‐tetra(methylene phosphonic acid) (DOTP) macrocyclic ligand. Two distinct homonuclear complexes were identified; the first was characterized by X‐ray crystallography as a unique “out‐of‐cage”, [U(DOTPH 6 ) 2 ] complex, in which the U IV cation is octa‐coordinated to 4 phosphonic arms from each ligand in a square anti‐prism geometry, with a C 4 symmetry. The second is the “in‐cage” [U(DOTPH 4 )] complex, in which the tetravalent cation is located between the macrocycle O 4 and N 4 planes. With the help of UV‐Vis absorption, 1 H/ 31 P NMR, ATR‐IR, and MALDI‐TOFMS analytical techniques, the chemical interchange between both species is presented. It is shown that the one‐way transition is governed by the formation of a multiple number of soluble oligomeric species consisting of varied stoichiometric ratios of both characterized homonuclear complexes." @default.
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• W3145645636 date "2021-05-07" @default.
• W3145645636 modified "2023-09-30" @default.
• W3145645636 title "Oligomers Intermediates in Between Two New Distinct Homonuclear Uranium(IV) DOTP Complexes**" @default.
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• W3145645636 doi "https://doi.org/10.1002/chem.202005350" @default.
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