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- W3146040160 abstract "(N-isopropylacrylamide )(PNIPAAm ) Thermoresponsive poly 刷浓密地 grafted 到经由开始表面的原子转移激进分子聚合(SI-ATRP ) 的硅石表面上。grafting 反应在 2-propanol 从 2-bromoisobutyratefunctionalized 硅石粒子的表面开始了在用 CuCl/CuCl2/N 的周围的温度的水的答案， N， N， N， N-pentamethyldiethylenetriamine (PMDETA ) 作为催化系统。把分析(TGA ) 基于 thermogravimetric 结果， grafting 数量和硅石的表面上的 PNIPAM 链的 grafting 密度被计算分别地是 1.29 mg/ m2 和 0.0215 chains/nm2。胶化浸透层析(GPC ) 结果显示出相对狭窄的分子的重量分发(M w/M n= 1.21 ) grafted PNIPAAm。修改硅石粒子作为包装材料成功地作为活动用水分开三芳香的混合物的高效的液体层析(HPLC ) 被使用由改变列温度的阶段。硅石粒子上的 PNIPAAm 刷子 grafted 的温度依赖者吸水 / 恐水病的性质改变与在静止阶段和 analytes 之间的色析法的相互作用被决定。保留时间被延长，分辨率与增加温度被改进。有在相对低的温度的高分辨率的基线分离被观察，证明稠密的 PNIPAAm 刷子是硅石表面上的 grafted。" @default.
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- W3146040160 date "2012-01-01" @default.
- W3146040160 modified "2023-09-23" @default.
- W3146040160 title "Preparation of poly（N-isopropylacrylamide） brush grafted silica particles via surface-initiated atom transfer radical polymerization used for aqueous chromatography" @default.
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