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- W3146518062 abstract "Reaction of [η5:σ-Me2C(C5H4)(C2B10H10)]Ru(NCCH3)2 (1) with R1C≡CR1(R1 = Et, Ph) in toluene at 80 °C yielded organoruthenium cyclobutadiene complexes [η5:σ-Me2C(C5H4)(C2B10H10)]Ru(-4-C4R14) in 80% yield. Treatment of 1 with diynes R2C≡C(CH2)3C≡CR2 (R2 = Me, Et) in toluene at room temperature yielded ruthenacyclopentatrienes [η5:σ-Me2C (C5H4)(C2B10H10)]Ru[=C2(R2)2C2(CH2)3] in 85% yield. These new complexes were fully characterized by various spectroscopic techniques, elemental analyses and single-crystal X-ray diffraction studies. The possible reaction mechanism was proposed." @default.
- W3146518062 created "2021-04-13" @default.
- W3146518062 creator A5039965896 @default.
- W3146518062 date "2010-01-01" @default.
- W3146518062 modified "2023-09-23" @default.
- W3146518062 title "Reaction of [η~5:σ-Me_2C(C_5H_4)(C_2B_(10)H_(10))]Ru(NCCH_3)_2 with internal alkynes:Synthesis and structural characterization of ruthenium-cyclobutadiene and ruthenacyclopentatriene complexes" @default.
- W3146518062 hasPublicationYear "2010" @default.
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