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- W3146620310 abstract "PEG 600 was used as phase-transfer catalyst to synthesize N, N-dimethyl-3-chloropropylamine Hydrochloride from dimethyl amine and 1-bromo-3-chloropropane. The effects of factors, such as the concentration of the catalyst of PEG 600, the mole ratio of dimethyl amine to 1-bromo-3-chloropropane, the reaction temperature and the reaction time on the yield, were examined. The optimal reaction conditions were determined as follows:the mole ratio of dimethyl amine to 1-bromo-3-chloropropane was 1. 2, PEG 600 catalyst was 2. 0 g, the reaction time was 4 h, the reaction temperature was 35~40 ℃, and the yield reached 73. 7%." @default.
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- W3146620310 date "2015-01-01" @default.
- W3146620310 modified "2023-09-27" @default.
- W3146620310 title "Synthesis of N,N-dimethyl-3-chloropropylamine Hydrochloride by Phase Transfer Catalysis" @default.
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