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- W3149761635 endingPage "117985" @default.
- W3149761635 startingPage "117985" @default.
- W3149761635 abstract "Elucidating the structure-activity relationship of curdlan is hampered by a lack of characterization with unique specific conformations (i.e., single- or triple-helix). In this study, single-helical curdlan is generated in dilute NaOH solutions at 35−50 °C, and characterized with NMR, SAXS, and GPC. The conformational transition from coil to single-helix and the intramolecular hydrogen bond interaction are explored using NMR. It is found that the two aforementioned types of curdlan interact with Congo Red in very different ways. Single-helical curdlan can encapsulate Congo Red to form a stable, supramolecular dye assembly, which is demonstrated by the shortest distance between the H3 of curdlan and the phenyl groups of Congo Red, and also the same self-diffusion coefficients of Congo Red and curdlan. In contrast, random-coil curdlan interacts weakly with Congo Red and cannot enwrap it. This study offers insight into the specific structure-activity relationship of beta-(1,3)-glucans." @default.
- W3149761635 created "2021-04-13" @default.
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- W3149761635 date "2021-07-01" @default.
- W3149761635 modified "2023-10-18" @default.
- W3149761635 title "Preparation and characterization of curdlan with unique single-helical conformation and its assembly with Congo Red" @default.
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- W3149761635 doi "https://doi.org/10.1016/j.carbpol.2021.117985" @default.
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