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- W3150255786 abstract "Abstract A method for total synthesis of thiangazole ( 1 ), a tris-thiazoline-oxazole metabolite, is described. The key intermediate 9 , a linear tetrapeptide amide composed of three S-benzyl-2-methylcysteine residues and a O-benzyl-threonine amide, was synthesized in 4 steps using 2-chloro-1,3-dimethyl-imidazolidium hexafluorophosphate(CIP)-mediated activation. The successive thiazoline/oxazole rings were constructed by TiCl 4 -mediated cyclodehydration followed by acid-catalyzed Robinson-Gabriel reaction without difficulty." @default.
- W3150255786 created "2021-04-13" @default.
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- W3150255786 date "2010-06-12" @default.
- W3150255786 modified "2023-09-24" @default.
- W3150255786 title "ChemInform Abstract: Total Synthesis of Thiangazole." @default.
- W3150255786 cites W2951646245 @default.
- W3150255786 doi "https://doi.org/10.1002/chin.199947241" @default.
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