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- W3150688006 abstract "Poly(methyl acrylate)-b-poly(5,6-benzo-2-methylene-1,3-dioxepane) (PMA-b-PBMDO) was synthesized by twostep atom transfer radical polymerization (ATRP). Firstly, ATRP of methyl acrylate (MA) was realized using ethyl α-bromobutyrate (EBrB) as initiator in the presence of CuBr/2,2'-bipyridine. After isolation, poly(methyl acrylate) with terminal bromine (PMA-Br) was synthesized. Secondly, the resulting PMA-Br was used as a macromolecular initiator in the ATRP of BMDO. The structure of block copolymer was characterized by 1H-NMR spectroscopy. Molecular weight and molecular weight distribution were determined on a gel permeation chromatograph (GPC)." @default.
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- W3150688006 date "2002-01-01" @default.
- W3150688006 modified "2023-09-24" @default.
- W3150688006 title "SYNTHESIS OF BLOCK COPOLYMER FROM 5,6-BENZO-2-METHYLENE-1,3-DIOXEPANE AND METHYL ACRYLATE VIA ATOM TRANSFER RADICAL POLYMERIZATION" @default.
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