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- W3151316363 abstract "Mesostructured nickel phosphate(MW-NiPO-2) was rapidly synthesized in the presence of cationic surfactant by a microwave assisted hydrothermal process.The synthesis parameters,microwave irradiation temperature and time,OH-/P and Ni/P molar ratios of the precursor,were systematically investigated and optimized.The characterizations of the materials obtained by the two different procedures,Sol-Gel method and microwave assisted hydrothermal process,were carried out by ICP,FT-IR,TEM and N2physisorption.The results show that MW-NiPO-2 can be obtained at relatively low temperature(60℃).When the microwave radiation temperature was 100℃,the mesostructured phase formed in an extremely short period about 0.25 h.Ordered MW-NiPO-2 can be obtained under microwave irradiation for 1 h at 100℃,when OH /P and the Ni/P molar ratios of the precursor are 2.0 and 0.7,respectively.In contrast,it took at least 24 h for completion via Sol-Gel method.MW-NiPO-2 and SG-NiPO-2 possess similar structure and composition while MW-NiPO-2 exhibites a worm-like appearance other than piled nanotubes.In comparison with the sample synthesized via Sol-Gel method,MW-NiPO-2 possesses a relatively high BET surface area(334.4 m2/g) and pore volume(0.318 cm3/g)." @default.
- W3151316363 created "2021-04-13" @default.
- W3151316363 creator A5065882197 @default.
- W3151316363 date "2012-01-01" @default.
- W3151316363 modified "2023-09-25" @default.
- W3151316363 title "Rapid Synthesis of Mesoporous Nickel Phosphates under Microwave Assisted Hydrothermal Condition" @default.
- W3151316363 hasPublicationYear "2012" @default.
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