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- W3151707586 abstract "The magnetic Fe3O4 nanoparticles were synthesized by co-precipitation method,and then magnetic Fe3O4@ Au nanoparticle was synthesized to improve the affinity of particle surface. L-Cys-GA3 was grafted on the surface of gold clad by self-assembly method,and then dropped it on glassy carbon electrode,for further manufacture of MIP /Fe3O4@ Au by using electropolymerzation L-Cys. The surface morphology and particle size distribution of Fe3O4@ Au were studied by TEM. The structure and composition of gibberellins A3,MIP and nMIP were studied by IR. The test system was optimized,and the results showed that when the cycles of electropolymerization was 30,acetic acid: methanol( 1 ∶ 8,V /V) was chosen as eluent,elution time was optimized for 5 min and rebinding time for 7 min,the sensor got a high stability and good recognition ability for gibberellins A3. The concentration of gibberellins A3 in the range of 1. 0 × 1011- 1. 0 × 108 mol /L had a relationship with the oxidation peak current of probe,with the detection limit of 2.57×1012mol /L. The sensor was successfully used for the determination of GA3 in beer sample." @default.
- W3151707586 created "2021-04-13" @default.
- W3151707586 creator A5050968602 @default.
- W3151707586 date "2014-01-01" @default.
- W3151707586 modified "2023-09-23" @default.
- W3151707586 title "Determination of Trace Gibberellin A3 by Magnetic Self-assembly Molecularly Imprinted Electrochemical Sensor" @default.
- W3151707586 hasPublicationYear "2014" @default.
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