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- W3152258105 abstract "A novel polyoxometalate-based composite compound [Ni(phen)2][Hphen](AsW12O40) (phen = 1,10-phenanthroline) 1 has been hydrothermally synthesized and characterized by elemental analysis, IR, TGA, ESR spectroscopy and single-crystal X-ray diffraction. Each structure unit of 1 consists of one polyoxoanion AsW12O403-, one free phenanthroline molecule and one coordination cation [Ni(phen)2]2+. The title compound crystallizes in the orthorhombic system, space group P212121, with a = 12.2383(7), b = 21.0884(11), c = 22.3237(12) , V = 5761.4(5) 3, Mr = 3520.44, Z = 4, Dc = 4.059 g/cm3, F(000) = 6204, μ(MoKα) = 24.844 mm-1, GOF = 1.022, the final R = 0.0376 and wR = 0.0742 (I 2σ(I)) for 865 parameters and 9637 observed reflections with I 2σ(I)." @default.
- W3152258105 created "2021-04-13" @default.
- W3152258105 creator A5089919376 @default.
- W3152258105 date "2007-01-01" @default.
- W3152258105 modified "2023-09-25" @default.
- W3152258105 title "Hydrothermal Synthesis and Crystal Structure of a Novel Composite Keggin-type Arsenotungstate: [Ni(phen)_2][Hphen](AsW_(12)O_(40))" @default.
- W3152258105 hasPublicationYear "2007" @default.
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